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Factory Supply industrial standard Diethyl dibutylmalonate 596-75-8 In Stock
- Molecular Formula: C15H28 O4
- Molecular Weight: 272.385
- Appearance/Colour: colourless liquid
- Vapor Pressure: 0.002mmHg at 25°C
- Refractive Index: n20/D 1.433(lit.)
- Boiling Point: 291 °C at 760 mmHg
- Flash Point: 126.4 °C
- PSA： 52.60000
- Density: 0.9457
- LogP: 3.47940
Diethyl dibutylmalonate(Cas 596-75-8) Usage
InChI:InChI=1/C15H28O4/c1-5-9-11-15(12-10-6-2,13(16)18-7-3)14(17)19-8-4/h5-12H2,1-4H3
596-75-8 Relevant articles
Method for preparing Guerbet acids by taking malonate as raw material
-
Paragraph 0024, (2017/08/29)
The invention discloses a method for pre...
Iron-catalyzed, hydrogen-mediated reductive cyclization of 1,6-enynes and diynes: Evidence for bis(imino)pyridine ligand participation
Sylvester, Kevin T.,Chirik, Paul J.
supporting information; experimental part, p. 8772 - 8774 (2009/12/04)
(Chemical Equation Presented) The bis(im...
Synthesis of 3-alkyl(aryl)thietanes
Shevchenko,Volynskii
body text, p. 123 - 128 (2010/02/28)
A preparative procedure for the synthesi...
Synthesis and Properties of New Lipophilic Macrotricyclic Cylindrical Cryptands
Quici, Silvio,Manfredi, Amedea,Raimondi, Laura,Sironi, Angelo
, p. 6379 - 6388 (2007/10/03)
Cylindrical cryptands 2a-c, in which two...
596-75-8 Process route
-
-
109-65-9
1-bromo-butane
-
-
105-53-3
diethyl malonate
-
-
596-75-8
diethyl dibutylmalonate
-
-
133-08-4
diethyl butylmalonate
| Conditions | Yield |
|---|---|
|
With
sodium ethanolate;
In
ethanol;
|
75%
4% |
|
tetrabutyl phosphonium bromide; potassium carbonate;
at 170 ℃;
under 20 Torr;
Product distribution;
other catalysts, other compounds, other products;
|
-
-
542-69-8
1-iodo-butane
-
-
105-53-3
diethyl malonate
-
-
596-75-8
diethyl dibutylmalonate
-
-
133-08-4
diethyl butylmalonate
| Conditions | Yield |
|---|---|
|
K2CO3+5percent Carbowax 6000;
at 170 ℃;
under 20 Torr;
Yield given. Yields of byproduct given;
|
596-75-8 Upstream products
-
109-65-9
1-bromo-butane
-
133-08-4
diethyl butylmalonate
-
542-69-8
1-iodo-butane
-
141-52-6
sodium ethanolate
596-75-8 Downstream products
-
24765-57-9
2,2-di-n-butylpropane-1,3-diol
-
17013-41-1
5,5-di-n-butylbarbituric acid
-
2283-16-1
di-n-butylmalonic acid
-
102887-77-4
2-Hydroxymethyl-2-butyl-hexanol-bis- <4-brom-benzolsulfonat>
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