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Chinese Factory Supply Wholesale 1,1'-Methylenedi-2-naphthol 1096-84-0 with Cheap Price
- Molecular Formula: C21H16 O2
- Molecular Weight: 300.357
- Appearance/Colour: light pink to light brown crystalline powder
- Melting Point: 181-190 °C (dec.)(lit.)
- Refractive Index: 1.5680 (estimate)
- Boiling Point: 543.4°Cat760mmHg
- PKA: 8.91±0.50(Predicted)
- Flash Point: 258.6°C
- PSA： 40.46000
- Density: 1.283g/cm3
- LogP: 4.99500
1096-84-0 Relevant articles
Reactions of naphthols with halogenmethanes under alkaline conditions
Brieskorn,Kallmayer
, p. 141 - 148 (1972)
-
Simplified synthesis of 1,1′[14C]-methylene-di (2-naphthol). A radiochemical and kinetic approach
Angelini, Giancarlo,Ursini, Ornella,Minetti, Patrizia,Celona, Diana,De Angelis, Francesco
, p. 543 - 556 (2004)
The synthesis of the 1,1′[14C]-methylene...
Dibromomethane as one-carbon source in organic synthesis: The Mannich base formation from the reaction of phenolic compounds with a preheated mixture of dibromomethane and diethylamine
Hon, Yung-Son,Chou, Yu-Yu,Wu, I-Che
, p. 2253 - 2267 (2004)
The salt formed from the reaction of dih...
Naphthalene Tetrachlorides and Related Compounds. Part 12. Influence of Some 1-Substituents on the Course of Chlorination of Derivatives of 2-Naphthol
Calvert, David J.,Mare, Peter B. D. de la,Suzuki, Hitomi
, p. 255 - 260 (1983)
The chlorinations of 1-methyl-2-naphthol...
Synthesis, characterization of the amido-conjugates of 1,1′- methylene-bis(2-naphthol) and recognition of Cu2+ in aqueous acetonitrile
Baghel, Garima Singh,Chinta, Jugun Prakash,Rao, Chebrolu P.
, p. 2397 - 2404 (2012)
Di-amido-derivatives of 1,1′-methylene-b...
Guest-Reaction Driven Cage to Conjoined Twin-Cage Mitosis-Like Host Transformation
Cai, Li-Xuan,Cheng, Pei-Ming,Hu, Shao-Jun,Li, Shao-Chuan,Sun, Qing-Fu,Yan, Dan-Ni,Zhou, Li-Peng
, p. 23569 - 23573 (2020)
We report here a guest-reaction-induced ...
Synthesis of dioxazaborocines from N-substituted-bis(2-hydroxyaryl)aminomethylamines
Woodgate, Paul D.,Horner, Gillian M.,Maynard, N. Paul,Rickard, Clifton E.F.
, p. 180 - 193 (1999)
The preparation of a number of tripodal ...
-
de Diesbach,Wanger,v. Stockalper
, p. 355,357 (1931)
-
Anticancer Activity and Catalytic Potential of Ruthenium(II)-Arene Complexes with N,O-Donor Ligands
Haghdoost, Mohammad Mehdi,Guard, Juliette,Golbaghi, Golara,Castonguay, Annie
, p. 7558 - 7567 (2018)
The special ability of organometallic co...
Reactivity of cis-bis(acetylacetonato)dichlorotitanium(IV) towards hydroxy-containing ligands: Isolation and characterisation of products
Rao, P. Venkateshwara,Rao, Chebrolu Pulla,Wegelius, Elina K.,Kolehmainen, Erkki,Rissanen, Kari
, p. 4469 - 4474 (1999)
The reactivity of cis-[Ti(acac)2Cl2] wit...
One-step novel synthesis of methylene bisphenols and methylene bisnaphthols using Lewis acid mediated rearrangement
Kumar, Sandeep,Mehta, Shilpika Bali
, (2021/12/20)
Mono- and di-substituted isomeric methyl...
ION CHANNEL ANTAGONISTS/BLOCKERS AND USES THEREOF
-
Page/Page column 22; 24; 25; 63; 64; 74-76; 78; 79, (2021/06/22)
Provided are ion channel antagonists/blo...
Ru-Catalyzed Selective Catalytic Methylation and Methylenation Reaction Employing Methanol as the C1 Source
Biswas, Nandita,Srimani, Dipankar
, p. 10544 - 10554 (2021/07/31)
Methanol can be employed as a green and ...
1096-84-0 Process route
-
-
C18 H21 NO
-
-
1096-84-0
bis(2-hydroxy-1-naphthyl)methane
-
-
3218-02-8
cyclohexylmethylamine
| Conditions | Yield |
|---|---|
|
With
sodium tetrahydroborate;
In
methanol;
at 20 ℃;
for 2h;
Schlenk technique;
Inert atmosphere;
|
|
|
Multi-step reaction
with
2
steps
1: sodium tetrahydroborate / methanol / 0.25 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
2: ethanol / 2 h / Inert atmosphere; Schlenk technique; Reflux
With
sodium tetrahydroborate;
In
methanol; ethanol;
|
-
-
C18 H23 NO
-
-
1096-84-0
bis(2-hydroxy-1-naphthyl)methane
-
-
3218-02-8
cyclohexylmethylamine
| Conditions | Yield |
|---|---|
|
In
ethanol;
for 2h;
Inert atmosphere;
Schlenk technique;
Reflux;
|
36%
|
1096-84-0 Upstream products
-
64-17-5
ethanol
-
100-97-0
hexamethylenetetramine
-
135-19-3
β-naphthol
-
33257-36-2
di-2-naphthoxymethane
1096-84-0 Downstream products
-
1076-26-2
1-methyl-2-naphthol
-
842-07-9
Sudan I
-
103328-07-0
1,1'-dihydroxy-1H ,1'H -1,1'-methanediyl-bis-naphthalen-2-one-bis-(4-nitro-phenylhydrazone)
-
115916-13-7
1,1'-dihydroxy-1H ,1'H -1,1'-methanediyl-bis-naphthalen-2-one-bis-(2,4-dinitro-phenylhydrazone)
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